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But, once you get back to Hyrule, you can't return to Outset Island and give them to Orca.

I don't think you can get spoils in the Salvage Labryinth. Of all the times I've been down there, none of the enemies dropped any goodies for me... But, then again, I haven't tested out my grappling hook on the enemies down there. I'll have to try that out. Edit: I tried it, it does work, but...